کتاب NMR حالت جامد در علم مواد: اصول و کاربردها (Solid-state NMR in materials science principles and applications)

کتاب NMR حالت جامد در علم مواد: اصول و کاربردها (Solid-state NMR in materials science principles and applications) برای افراد غیر متخصص نوشته شده است و شامل اصول تئوری و عملی ثبت سیگنال‌های طیف سنجی NMR همراه با معرفی تجهیزات مختلف NMR است.

این کتاب پس از مقدمه، شامل موارد زیر است:

• تئوری و ویژگی های NMR حالت جامد و آسایش هسته ای در جامدات، از جمله دینامیک مواد
• بررسی مواد مختلف دیامغناطیس و پارامغناطیس، شامل فلزات و خوشه های فلزی تاکامپوزیت های آمورف
• روش‌شناسی جمع‌آوری و تفسیر داده‌های NMR حالت جامد، از جمله استراتژی‌ها و معیارها برای توصیف خصوصیات ساختاری مواد مختلف
• نمونه‌های عملی آزمایش‌های NMR و آرامش چند هسته‌ای و همچنین تفسیر داده‌های به‌دست‌آمده
• آزمایش‌های متعدد NMR حالت جامد برای مواد مختلف برای ارزیابی ساختار و دینامیک آنها
  کتاب Solid-state NMR in materials science principles and applications به زبانی روشن و ساده نوشته شده است و شامل تصاویر واضح، مثال‌های متعدد و مراجع مفصل است. این کتاب یک مرجع عالی نه تنها برای محققان جوان و با تجربه، بلکه برای دانشجویان علاقه مند به آینده  علم مواد و شیمی است.

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  Table of Contents
  General Principles of Pulsed NMR and NMR Techniques
  Early History of NMR in the Solid State
  Nuclei in the External Magnetic Field
  Effects of Radio Frequency Pulses
  From Macroscopic Magnetization to Nuclear Relaxation and Shapes of NMR Signals
  Parameters Characterizing Nuclei in the External Magnetic Field
  Introducing NMR Equipment and NMR Experiments
  Main Principles of Two-Dimensional NMR
  Enhancement of Sensitivity in NMR

  On Amorphous Materials as Potential Objects in Solid-State NMR Studies: Common and Key Problems
  Hybrid Materials
  Polymer Solids
  Systems Based on Nanostructures
  Wood and Wood Components
  Glasses
  Zeolites
  Design of Porous and Layered Molecular Systems

  Features of Solid-State NMR: Diamagnetic Materials
  From Isotropic Chemical Shifts to Magnetic Shielding Tensors
  Nuclei with a Spin of 1/2
  Quadrupolar Nuclei in Solids
  Detection of NMR Signals in Solids: Common Aspects
  High-Power Decoupling
  Multi-Quantum NMR Experiments
  Dipolar Recoupling NMR Techniques
  Sideband Manipulations
  Zero-Field Solid-State NMR Experiments
  Solid-State NMR Imaging

  Practice of Multinuclear NMR in Diamagnetic Solids: General Information and Examples of Applications
  Structural Information by Increasing the Spectral Resolution in Multinuclear Solid-State NMR
  Probing Proximities of Nuclei and Measurements of Internuclear Distances in Diamagnetic Solids
  31P Solid-State NMR
  Solid-State NMR of Halogen Nuclei and Oxygen
  Solid-State NMR of Oxide Materials: Nuclei 51V, 93Nb, and 181Ta
  Solid-State 13C NMR: Wood and Wood Products
  2H NMR in Solids at Deuterium Natural Abundance
  Between Solution- and Solid-State NMR: Nanoparticles and Suspensions

  Dynamics in Diamagnetic Materials from Solid-State NMR: Methods, Measurements, and Analysis
  Variable-Temperature Solid-State NMR Experiments and a Line-Shape Analysis
  Molecular Mobility from the Solid-State NMR Relaxation
  One- and Two-Dimensional Exchange Solid-State NMR Spectroscopy
  Molecular Mobility from the Cross-Polarization NMR Experiments
  Molecular Mobility from Magnetic Relaxation Dispersion Experiments

  Strategies in Solid-State Multinuclear NMR: Studies of Diamagnetic Porous Materials
  Porosity of Materials from NMR
  Structural Features of Silica Lattice and Surface by Solid-State 1H 29Si, 27Al, and 17O NMR Spectra
  Molecular Mobility in Diamagnetic Porous Materials

  Paramagnetic Effects in Solid-State NMR
  Theoretical Aspects
  Nuclear Relaxation in the Presence of Unpaired Electrons
  Practical Consequences from the Theory of Paramagnetic Effects
  1H, 31P, 13C, 2H, 29Si, 7Li, and 6Li NMR Spectra of Paramagnetic Solids
  51V and 55Mn NMR Spectra of Paramagnetic Solids
  Special NMR Techniques for Observations of “Invisible” Target Nuclei
  Relaxation Measurements and Relaxation Times in Paramagnetic Solids

  Strategy in NMR Studies of Amorphous Porous Paramagnetic Materials
  Intense Sideband Patterns in MAS NMR Spectra of Paramagnetic Amorphous Materials and Their Analysis
  Direct Detection of the Nuclei Closest to Paramagnetic Ions in Porous Materials by the Hahn-Echo Mapping NMR Experiments
  NMR Relaxation Approaches to Structure of Porous Amorphous Paramagnetic Silica-Based Materials: From Experiments to Models and Interpretations
  Protocol for Quantification of “Invisible Nuclei” in MAS NMR
  Concluding Remarks